ASTM-C791:2012 Edition

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C791-12 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Boron Carbide

Published By	Publication Date	Number of Pages
ASTM	2012	26

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Categories: 27.120.30 - Fissile materials and nuclear fuel technology, ASTM

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Description

1.1 These test methods cover procedures for the chemical, mass spectrometric, and spectrochemical analysis of nuclear-grade boron carbide powder and pellets to determine compliance with specifications.

1.2 The analytical procedures appear in the following order:

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents Significance and Use Reagents Safety Precautions Sampling
2	Scope Summary of Test Method Interferences Apparatus Reagents Sampling and Sample Preparation Calibration Procedure
3	Calculation ( ) Scope Summary of Method Interferences
4	Apparatus Reagents Precautions Sampling and Sample Preparation Procedure
5	Titrimetric Determination of Boron
6	ICP OES
7	Precision and Bias Scope Summary of Method Interferences Isotopic Composition by TIMS
8	Isotopic Composition by ICP MS
9	Scope Summary of Method Interferences Apparatus Reagents Precautions Procedure
10	Pyrohydrolysis as Sample Preparation Procedure for Isotipic Composition by ICP MS Scope Summary of Method
11	Interferences Apparatus Reagents Calibration of Titrator Procedure Calculation Precision and Accuracy Scope Summary of Method
12	Interferences Apparatus Reagents Calibration of Electrode Procedure Calculation Precision and Accuracy Preface
13	Scope Water by Constant-Voltage Coulometry
14	Weight Loss on Drying Method
15	DCArc OES Method
16	Wet Chemical Methods
17	Scope Summary of Method Interferences
18	Apparatus Reagents Precautions Standardization of Titrant Blank Sample Preparation Procedure
19	Calculation Procedure Calculation Precision and Bias
20	Determination of Soluble Boron by ICP OES Scope Summary of Method Interferences Apparatus
21	Reagents Sample Preparation Calibration Procedure Calculation of Free Carbon Content
22	Precision and Bias A1. Commercial Reference Materials REFERENCES
23	TABLE 1
24	FIG. 1 FIG. 2
25	FIG. 3
26	FIG. 4

Additional information

	Sections
Total Carbon by Combustion in an Inductive Furnace and Infrared Measurement	7-16
Chloride by Constant-Current Coulometry	41-49
Isotopic Composition by Mass Spectrometry	28-32
Pyrohydrolysis	33-40
Total Boron by Titrimetry and ICP OES	17-27
Soluble Boron by Titrimetry and ICP OES	65-79
Water by Constant-Voltage Coulometry and Weight Loss on Drying	59-62
Free Carbon by a Coulometric Method	80-89
Chloride and Fluoride by Ion-Selective Electrode	50-58
Metallic Impurities	63 and 64
ICS Codes	27.120.30 - Fissile materials and nuclear fuel technology

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ASTM-C791:2012 Edition

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