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ASTM-D4671:2010 Edition

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D4671-05(2010)e1 Standard Test Method for Polyurethane Raw Materials Determination of Unsaturation of Polyols

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ASTM 2010 4
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1.1 These test methods measure unsaturation in polyether polyols. (See Note 1.)

1.1.1 Test Method A, High-Volume Reagent Method Uses about 50 mL of 0.1 M mercuric acetate reagent in methanol and 15 g or more of sample. These test methods use an indicator for colorimetric determination of an end point. It is recommended for polyols with low values (below 0.01 millequivalents per gram (meq/g)) of unsaturation where large sample sizes are required.

1.1.2 Test Method B, Low-Volume Reagent Method Uses 2 mL of ca. 0.05 M mercuric acetate reagent in methanol and about 1 g of sample or less. These test methods use a potentiometric determination of an end point.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Note 1There is no known ISO equivalent to this standard.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
Summary of Test Method
Significance and Use
Interferences
2 Apparatus
Reagents
Procedure
Calculation
Precision and Bias
Apparatus
3 Reagents
Procedure
Calculation
Report
Precision and Bias
TABLE 1
4 Keywords
TABLE 2
ASTM-D4671
$35.75