ASTM-D501:2016 Edition
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D501-03(2016) Standard Test Methods of Sampling and Chemical Analysis of Alkaline Detergents
Published By | Publication Date | Number of Pages |
ASTM | 2016 | 27 |
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ASTM D501-03-Reapproved2016
Historical Standard: Standard Test Methods of Sampling and Chemical Analysis of Alkaline Detergents
ASTM D501
Scope
1.1 These test methods cover procedures for the sampling and chemical analysis of inorganic alkaline detergents.
1.2 The procedures appear in the following order:
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage.
Keywords
alkaline builder; borax; caustic soda; detergent; ignition loss; insoluble; particle size; phosphate; silicate; soda ash; turbidity ;
ICS Code
ICS Number Code 71.100.40 (Surface active agents)
DOI: 10.1520/D0501-03R16
Trisodium Phosphate Calculated as Na3PO4·12H2O, Na3PO4· H2O, Na3PO4, and as P2O5 | 65 – 68 |
---|---|
Sulfate | 135 – 137 |
Turbidity | 129 |
Sodium Bicarbonate: | |
Reverse-Flow Ion-Exchange Chromatography (Preferred Method) | 108 – 119 |
Matter Volatile at 150 to 155°C | 18 and 19 |
Sodium Bicarbonate, Sodium Carbonate, and Free Moisture | 42 – 45 |
Carbon Dioxide (CO2) by the Evolution Method | 13 – 16 |
Total Alkalinity as Sodium Carbonate (Na2CO3 ) | 20 – 22 |
Borax: | |
Total Borate and Excess Alkalinity or Acidity | 85 – 87 |
Carbonate as Sodium Carbonate (Na2CO3) | 12 |
Sodium Metasilicate (Na2SiO3·5H2O) | 54 |
Sodium Bicarbonate (NaHCO3) by Potentiometric Titration | 26 – 28 |
Sodium Metasilicate, Sodium Sesquisilicate and Sodium Orthosil- icate: | |
Paper Chromatographic Method | 120 – 127 |
Temperature Rise | 130 – 134 |
Sodium Sesquisilicate (3Na2O·2SiO2·11H2O) | 55 |
Tetrasodium Pyrophosphate: | |
Sodium Triphosphate: | |
Sodium Bicarbonate (NaHCO3) and Sodium Carbonate (Na2CO3) | 37 – 39 |
Alternative Method | 98 – 101 |
Tritratable Na2O | 91 – 94 |
pH of 1 percent Solution | 128 |
Preferred Method | 95 – 97 |
Particle Size | 145 |
Loss on Ignition of Sodium Sesquisilicate (3Na2O·2SiO2 ·11H2O) | 58 and 59 |
Loss on Ignition | 82 and 83 |
pH Titration | 102 – 107 |
Total Alkalinity as Sodium Oxide (Na2O) | 69 – 71 |
Soda Ash: | |
Ignition Loss | 140 and 141 |
Apparent Density | 31 and 32 |
Trisodium Phosphate: | |
Orthophosphate | 146 – 151 |
Sodium Hydroxide (NaOH) | 9 – 11 |
Modified Soda (Sequicarbonate Type): | |
Sodium Bicarbonate (NaHCO3) | 23 – 25 |
Matter Insoluble in Water | 142 – 144 |
Sodium Orthosilicate (Na4SiO4) | 60 |
Total Silica as SiO2 | 51 – 53 |
Sampling | 90 |
Tetrasodium Pyrophosphate (Na4P2O7) | 75 – 79 |
Caustic Soda: | |
Total P2O5: | |
Trisodium Phosphate (Na3PO4) Content and Phosphorus Pentoxide (P2O5) | 62 – 64 |
Quantitative Separation and Measurement of Various Phosphates: | |
ICS Codes | 71.100.40 - Surface active agents |
Sections |
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