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ASTM-D5011:2003 Edition

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D5011-92(2003) Standard Practices for Calibration of Ozone Monitors Using Transfer Standards

Published By Publication Date Number of Pages
ASTM 2003 28
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1.1 These practices describe means for calibrating ambient, workplace or indoor ozone monitors, using transfer standards.

1.2 These practices describe five types of transfer standards: (A) Analytical instruments (B) Boric acid potassium iodide (BAKI) manual analytical procedure (C) Gas phase titration with excess nitric oxide (D) Gas phase titration with excess ozone (E) Ozone generator device.

1.3 These practices describe procedures to establish the authority of transfer standards: qualification, certification, and periodic recertification.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 8 for specific precautionary statements.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
2 Summary of Practices
3 Significance and Use
Apparatus
FIG. 1
4 FIG. 2
5 Reagents and Materials
FIG. 3
6 Hazards
Establishing the Authority of Transfer Standards
7 FIG. 4
8 Qualification Tests
9 FIG. 5
FIG. 6
11 Procedure for Certification
FIG. 7
12 FIG. 8
13 FIG. 9
FIG. 10
14 Recertification
FIG. 11
FIG. 12
15 Keywords
A1. SPECIFICATION FOR OZONE TRANSFER STANDARDS
A1.1
FIG. 13
16 A1.2
A1.3
A1.4 Recertification
A1.5 Transfer Standards Having Fewer Than Five Discrete Outputs
17 A2. CERTIFICATION OF THE BORIC ACID POTASSIUM IODIDE PROCEDURE AS A TRANSFER STANDARD
A2.1
A2.2
A2.3
A2.4 Potassium Iodide Calibration Curve
A2.5 Calibration of the O3 Generator
FIG. A2.1
18 A2.6 Certification as a Transfer Standard
A2.7 Calibration of the O3 Monitor
19 A3. CERTIFICATION OF THE GAS PHASE TITRATION WITH EXCESS NITRIC OXIDE PROCEDURE AS A TRANSFER STANDARD
A3.1 Dynamic Parameter Specifications
A3.2 Procedure
FIG. A2.2
20 A3.3 Calibration of the NO Monitor
A3.4 Calibration of the O3 Generator
A3.5 Certification as a Transfer Standard
A3.6 Calibration of the O3 Monitor
21 A3.7 Options
A4. CERTIFICATION OF THE GAS PHASE TITRATION WITH EXCESS OZONE PROCEDURE AS A TRANSFER STANDARD
A4.1 Dynamic Parameter Specifications
A4.2
A4.3 Procedure
23 A5. ALTERNATE PROCEDURES TO COMPARE A GENERATION-TYPE TRANSFER STANDARD TO A UV PRIMARY OZONE STANDARD
A5.1
A5.2
A5.3
FIG. A5.1
24 A6. CERTIFICATION OF AN OZONE MONITOR AS A TRANSFER STANDARD
A6.1
FIG. A5.2
25 A6.2 Preliminary Requirements
A6.3 Qualification
A6.4 Qualification Tests
A6.5 Certification
26 A6.6
A7. CERTIFICATION OF AN OZONE GENERATOR AS A TRANSFER STANDARD
A7.1 Preliminary Requirements
A7.2 Qualification
A7.3 Qualification Tests
27 A7.4 Certification
A7.5
REFERENCES
ASTM-D5011
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