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ASTM-F1593:2008 Edition

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F1593-08 Standard Test Method for Trace Metallic Impurities in Electronic Grade Aluminum by High Mass-Resolution Glow-Discharge Mass Spectrometer

Published By Publication Date Number of Pages
ASTM 2008 7
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1.1 This test method covers measuring the concentrations of trace metallic impurities in high purity aluminum.

1.2 This test method pertains to analysis by magnetic-sector glow discharge mass spectrometer (GDMS).

1.3 The aluminum matrix must be 99.9 weight % (3N-grade) pure, or purer, with respect to metallic impurities. There must be no major alloy constituent, for example, silicon or copper, greater than 1000 weight ppm in concentration.

1.4 This test method does not include all the information needed to complete GDMS analyses. Sophisticated computer-controlled laboratory equipment skillfully used by an experienced operator is required to achieve the required sensitivity. This test method does cover the particular factors (for example, specimen preparation, setting of relative sensitivity factors, determination of sensitivity limits, etc.) known by the responsible technical committee to affect the reliability of high purity aluminum analyses.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
Summary of the Test Method
2 Significance and Use
Apparatus
Reagents and Materials
Preparation of Reference Standards and Test Specimens
TABLE 1
3 Preparation of the GDMS Apparatus
Instrument Quality Control
Standardization
Procedure
TABLE 2
4 Detection Limit Determination
TABLE 3
5 GDMS Analysis for Thorium, Uranium, and Similar Elements
Report
Precision and Bias
FIG. 1
FIG. 2
6 Keywords
TABLE 4
7 A1. MASS SPECTRUM INTERFERENCES
A1.1
ASTM-F1593
$40.63