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ASTM-F2013:2005 Edition

ASTM-F2013:2005 Edition

$40.63

F2013-05 Standard Test Method for Determination of Residual Acetaldehyde in Polyethylene Terephthalate Bottle Polymer Using an Automated Static Head-Space Sampling Device and a Capillary GC with a Flame Ionization Detector

Published By Publication Date Number of Pages
ASTM 2005 9
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ASTM F2013-05

Historical Standard: Standard Test Method for Determination of Residual Acetaldehyde in Polyethylene Terephthalate Bottle Polymer Using an Automated Static Head-Space Sampling Device and a Capillary GC with a Flame Ionization Detector

ASTM F2013

Scope

1.1 This test method covers a gas chromatographic procedure for the determination of the ppm residual acetaldehyde (AA) present in poly(ethylene terephthalate) (PET) homo-polymers and co-polymers which are used in the manufacture of beverage bottles. This includes sample types of both amorphous and solid-stated pellet and preform samples, as opposed to the bottle test, Test Method D 4509, an acetaldehyde test requiring 24 h of desorption time at 23Ā°C into the bottle headspace and then the concentration of the headspace quantified by a similar GC method.

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Keywords

AA test; acetaldehyde; carbonated soft drink; ground parison AA; PET bottles; 24 hours headspace; water

ICS Code

ICS Number Code 55.100 (Bottles. Pots. Jars)

DOI: 10.1520/F2013-05

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
Summary of Test Method
Significance and Use
Sources of Error
2 Apparatus
Reagents and Materials
Calibration and Standardization
Sample Preparation
Procedure
3 Calculation
Report
Precision and Bias
4 Keywords
X1. HEWLETT-PACKARD 6890 SERIES GC CONDITIONS
X2. HEWLETT-PACKARD 7694 HEAD-SPACE SAMPLER CONDITIONS
TABLE X1.1
TABLE X2.1
5 X3. HEWLETT-PACKARD 6890 SERIES INTEGRATOR METHOD FILE
FIG. X3.1
6 FIG. X3.1
7 FIG. X3.1
8 X4. CHROMATOGRAM OF A TYPICAL SAMPLE
X5. PREPARATION OF ACETALDEHYDE CALIBRATION STANDARDS
X5.1 Introduction
X5.2 Materials
FIG. X4.1
9 X5.3 Setup
X5.4 Procedure
X5.5 Labeling

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