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BS EN 1427:2015

$102.76

Bitumen and bituminous binders. Determination of the softening point. Ring and Ball method

Published By Publication Date Number of Pages
BSI 2015 22
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This European Standard specifies a method for the determination of the softening point of bitumen and bituminous binders in the range of 28 °C to 150 °C.

Technical warning – The change from mercury thermometers to electronic temperature devices has revealed that the temperature definition in the mercury thermometer has not been precise enough to make a correct, unbiased transfer to electronic devices. Care should be taken for softening points ring and ball above 100 °C as the condition may have changed from previous practise to present days testing equipment. Below approx. 100 °C the difference in temperature readings between electronic and mercury stem thermometer is acceptable compared to the repeatability of this test methods. [Reference: ASTM E20 Group]

NOTE

The method described is also applicable to bituminous binders that have been recovered from bituminous mixes, e.g. by extraction.

WARNING —

Use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages PDF Title
5 Foreword
6 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials
5.1 General
7 5.2 Bath liquid
5.2.1 Distilled or deionized water
5.2.2 Glycerol, with a density (1 250 ± 10) kg/m3 at 20 C, with a 99 % mass fraction purity.
5.3 Release agent, mixture of glycerol and dextrin or mineral talc, or another commercially available release agent.
6 Apparatus
6.1 Ring and Ball apparatus,
8 6.2 Calibration/Verification
9 7 Preparation and preservation of laboratory samples and test samples
8 Procedure and reporting
11 9 Expression of results
10 Precision
10.1 Repeatability
10.2 Reproducibility
Table 1 — Precision
12 11 Test report
13 Figure 3 — Ball centering guide (examples)
14 Figure 4 — Ring holder (A)
16 Annex A (informative) Characteristics of thermometers
17 Annex B (informative) Examples of valid and invalid temperature gradients
B.1 Examples
B.1.1 General
B.1.2 Example 1 Bath liquid: Water
Table B.1 — Examples of valid and invalid temperature gradient for water as bath liquid. Invalid part of Test 2 is shown in bold letters
18 B.1.3 Example 2 Bath liquid: Glycerol
Table B.2 — Example of valid temperature gradient for glycerol as bath liquid
19 Table B.3 — Example of invalid temperature gradient for water as bath liquid. Invalid part of Test 2 is shown in bold letters
20 Bibliography
BS EN 1427:2015
$102.76