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BS ISO 13312:2017

$102.76

Iron ores. Determination of potassium. Flame atomic absorption spectrometric method

Published By Publication Date Number of Pages
BSI 2017 20
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This document specifies a flame atomic absorption spectrometric method for the determination of the mass fraction of potassium in iron ores.

This method is applicable to mass fractions of potassium between 0,002 5 % and 0,52 % in natural iron ores, iron ore concentrates and agglomerates, including sinter products.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
8 5 Reagents
6 Apparatus
10 7 Sampling and samples
7.1 Laboratory sample
7.2 Preparation of predried test samples
8 Procedure
8.1 Number of determinations
8.2 Test portion
8.3 Blank test and check test
11 8.4 Determination
8.4.1 General
8.4.2 Decomposition of the test portion
8.4.3 Treatment of the solution
8.4.4 Preparation of the set of calibration solutions
12 8.4.5 Adjustment of atomic absorption spectrometer
8.4.6 Atomic absorption measurements
9 Expression of results
9.1 Calculation of mass fraction of potassium
13 9.2 General treatment of results
9.2.1 Repeatability and permissible tolerance
9.2.2 Determination of analytical result
9.2.3 Between-laboratories precision
14 9.2.4 Check for trueness
15 9.2.5 Calculation of final result
9.3 Oxide factor
10 Test report
16 Annex A (normative) Flowsheet of the procedure for the acceptance of analytical values for test samples
17 Annex B (informative) Derivation of repeatability and permissible tolerance formulae
18 Annex C (informative) Precision data obtained by international analytical trials
19 Bibliography
BS ISO 13312:2017
$102.76