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BS ISO 14707:2021

$102.76

Surface chemical analysis. Glow discharge optical emission spectrometry (GD-OES). Introduction to use

Published By Publication Date Number of Pages
BSI 2021 22
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This document provides guidelines that are applicable to bulk and depth profiling GD-OES analyses. The guidelines discussed herein are limited to the analysis of rigid solids, and do not cover the analysis of powders, gases or solutions. Combined with specific standard methods which are available now and, in the future, these guidelines are intended to enable the regulation of instruments and the control of measuring conditions.

Although several types of glow discharge optical emission sources have been developed over the years, the Grimm type with a hollow anode accounts for a very large majority of glow discharge optical emission devices currently in use both for dc and rf sources. However, the cathode contact is often located at the back of the sample, in e.g. the Marcus type source, rather than at the front as in the original Grimm design. The guidelines contained herein are equally applicable to both and other source designs and the Grimm type source is used only as an example.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
10 4 Principle
5 Apparatus
5.1 Glow discharge optical emission source
13 5.2 Optical unit
5.3 Photoelectric detectors and measuring devices
6 Procedure
6.1 Verification tests of apparatus
6.1.1 General
14 6.1.2 Glow discharge source
15 6.1.3 Optical unit and electric measuring device
6.2 Determination
6.2.1 General
6.2.2 Preparation of the required calibration specimens
16 6.2.3 Setting up of measuring conditions and analysis of specimens
6.2.4 Quality check of results
6.2.5 Test report
18 Annex A (informative) Safety
20 Bibliography
BS ISO 14707:2021
$102.76