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BS ISO 16000-3:2022

$167.15

Indoor air – Determination of formaldehyde and other carbonyl compounds in indoor and test chamber air. Active sampling method

Published By Publication Date Number of Pages
BSI 2022 36
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PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
10 4 Principle
5 Limitations and interferences
5.1 General
11 5.2 Ozone interference
12 6 Safety measures
7 Apparatus
7.1 Sampling
7.2 Sample preparation
14 7.3 Sample analysis
15 8 Reagents and materials
9 Preparation of reagents and cartridges
9.1 Purification of 2,4-dinitrophenylhydrazine
16 9.2 Preparation of DNPH formaldehyde derivative
9.3 Preparation of DNPH formaldehyde standards
17 9.4 Preparation of DNPH coated silica gel cartridges
9.4.1 General
9.4.2 DNPH coating solution
9.4.3 Coating of silica gel cartridges
18 10 Procedure
10.1 Sample collection
20 10.2 Process blanks
10.3 Sample analysis
10.3.1 Sample preparation
10.3.2 Sample desorption
10.3.3 HPLC calibration
23 10.3.4 HPLC analysis for formaldehyde
25 10.3.5 HPLC analysis of other aldehydes and ketones
27 11 Calculations
28 12 Performance criteria and quality assurance
12.1 General
12.2 Standard operating procedures (SOPs)
12.3 HPLC system performance
29 12.4 Sample loss
12.5 Measurement plan
13 Precision and uncertainty
14 Test report
31 Annex A (informative) Melting points of DNPH carbonyl derivatives
32 Annex B (informative) Precision and uncertainty
34 Bibliography
BS ISO 16000-3:2022
$167.15