BS ISO 22634-1:2019

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Cigarettes. Determination of benzo[a]pyrene in cigarette mainstream smoke using GC/MS – Method using methanol as extraction solvent

Published By	Publication Date	Number of Pages
BSI	2019	20

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Description

This document specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter (TPM) of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC/MS) with methanol as extraction solvent.

This method is specified using ISO 3308 smoking parameters. An alternative method for the determination of B[a]P is specified in ISO 22634-2 with a different clean-up using cyclohexane solvent and a shorter total analytical time.

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PDF Pages	PDF Title
2	National foreword
6	Foreword
7	Introduction
9	1 Scope 2 Normative references 3 Terms and definitions 4 Principle
10	5 Apparatus 6 Reagents
11	7 Standards 7.1 General 7.2 Primary B[a]P stock solution 7.3 Secondary B[a]P stock solution 7.4 B[a]P-d12 stock solution 7.5 B[a]P-d12 spiking solution 7.6 Working standard solutions 7.7 Storage of standard solutions
12	8 Preparation of sample 8.1 Sampling 8.2 Smoking 8.3 Glass-fibre filter pad extraction 8.4 Sample clean-up
13	9 Determination 9.1 GC/MS operating conditions
14	9.2 Calibration 9.3 Determination of B[a]P 9.4 Calculation 10 Repeatability and reproducibility
15	11 Test report 11.1 General 11.2 Characteristic data about the cigarette 11.3 Data about sampling
16	11.4 Description of the test 11.5 Test results
17	Annex A (informative) Example of a chromatogram of a cigarette smoke extract
19	Bibliography

Additional information

Status	Definitive
Pages	20
Publication Date	2019-12-06
ISBN	978 0 539 03141 6
Standard Number	BS ISO 22634-1:2019
Title	Cigarettes. Determination of benzo[a]pyrene in cigarette mainstream smoke using GC/MS – Method using methanol as extraction solvent
Identical National Standard Of	ISO 22634-1
Replaces	BS ISO 22634-1:2017
Descriptors	Aromatic hydrocarbons, Cigarettes, Determination of content, Mass spectrometry, Gas chromatography, Tobacco testing, Tobacco, Cyclic compounds, Smoke, Chemical analysis and testing
Publisher	BSI
Committee	AW/40
ICS Codes	65.160 - Tobacco, tobacco products and related equipment

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BS ISO 22634-1:2019

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