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BS ISO 23906-1:2020

$102.76

Cigarettes. Determination of benzo[a]pyrene in cigarette mainstream smoke with an intense smoking regime using GC/MS – Method using methanol as extraction solvent

Published By Publication Date Number of Pages
BSI 2020 20
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This document specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter (TPM) of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC-MS) with methanol as extraction solvent.

This method is specified using ISO 20778 smoking parameters.

NOTE

An alternative method for the determination of B[a]P is specified in ISO 23906-2 with a different clean-up using cyclohexane solvent and a shorter total analytical time.

PDF Catalog

PDF Pages PDF Title
2 undefined
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
10 4 Principle
5 Apparatus
6 Reagents
11 7 Standards
7.1 General
7.2 Primary B[a]P stock solution
7.3 Secondary B[a]P stock solution
7.4 B[a]P-d12 stock solution
7.5 B[a]P-d12 spiking solution
7.6 Working standard solutions
7.7 Storage of standard solutions
12 8 Preparation of sample
8.1 Sampling
8.2 Smoking
8.3 Glass-fibre filter pad extraction
8.4 Sample clean-up
13 9 Determination
9.1 GC-MS operating conditions
14 9.2 Calibration
9.3 Determination of B[a]P
9.4 Calculation
10 Repeatability and reproducibility
15 11 Test report
11.1 General
16 11.2 Characteristic data about the cigarette
11.3 Data about sampling
11.4 Description of the test
11.5 Test results
17 Annex A (informative) Example of a chromatogram of a cigarette smoke extract
19 Bibliography
BS ISO 23906-1:2020
$102.76