BS ISO 23906-1:2020
$102.76
Cigarettes. Determination of benzo[a]pyrene in cigarette mainstream smoke with an intense smoking regime using GC/MS – Method using methanol as extraction solvent
Published By | Publication Date | Number of Pages |
BSI | 2020 | 20 |
This document specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter (TPM) of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC-MS) with methanol as extraction solvent.
This method is specified using ISO 20778 smoking parameters.
An alternative method for the determination of B[a]P is specified in ISO 23906-2 with a different clean-up using cyclohexane solvent and a shorter total analytical time.
PDF Catalog
PDF Pages | PDF Title |
---|---|
2 | undefined |
6 | Foreword |
7 | Introduction |
9 | 1 Scope 2 Normative references 3 Terms and definitions |
10 | 4 Principle 5 Apparatus 6 Reagents |
11 | 7 Standards 7.1 General 7.2 Primary B[a]P stock solution 7.3 Secondary B[a]P stock solution 7.4 B[a]P-d12 stock solution 7.5 B[a]P-d12 spiking solution 7.6 Working standard solutions 7.7 Storage of standard solutions |
12 | 8 Preparation of sample 8.1 Sampling 8.2 Smoking 8.3 Glass-fibre filter pad extraction 8.4 Sample clean-up |
13 | 9 Determination 9.1 GC-MS operating conditions |
14 | 9.2 Calibration 9.3 Determination of B[a]P 9.4 Calculation 10 Repeatability and reproducibility |
15 | 11 Test report 11.1 General |
16 | 11.2 Characteristic data about the cigarette 11.3 Data about sampling 11.4 Description of the test 11.5 Test results |
17 | Annex A (informative) Example of a chromatogram of a cigarette smoke extract |
19 | Bibliography |