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BS ISO 8332:2018 – TC:2020 Edition

$217.84

Tracked Changes. Rubber compounding ingredients. Sulfur. Methods of test

Published By Publication Date Number of Pages
BSI 2020 71
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PDF Catalog

PDF Pages PDF Title
37 undefined
42 Foreword
43 Introduction
44 1 Scope
2 Normative references
3 Terms and definitions
4 Physical and chemical properties
45 5 Determination of total sulfur content
5.1 Principle
5.2 Reagents
5.3 Procedure
46 5.4 Expression of results
5.5 Precision
6 Determination of sieve residue
6.1 Principle
47 6.2 Method A
6.2.1 Apparatus
48 6.2.2 Procedure
6.2.3 Expression of results
49 6.3 Method B
6.3.1 Apparatus
6.3.2 Procedure
6.3.3 Expression of results
6.3.4 Precision
50 7 Determination of oil content of oil-treated sulfur
7.1 Principle
7.2 Hexane procedure
7.2.1 Reagents
7.2.2 Procedure
7.2.3 Expression of results
51 7.3 Sulfur-saturated hexane procedure
7.3.1 Reagents
7.3.2 Procedure
7.3.3 Expression of results
8 Determination of insoluble-sulfur content
8.1 Principle
52 8.2 Reference procedure using toluene
8.2.1 Reagents
8.2.2 Procedure
8.2.3 Expression of results
8.3 Alternative procedure using carbon disulfide
8.3.1 Reagents
53 8.3.2 Procedure
8.3.3 Expression of results
9 Determination of thermal reversion of insoluble sulfur
9.1 General
54 9.2 Method A
9.2.1 Principle
9.2.2 Apparatus
9.2.3 Reference procedure
56 9.2.4 Alternative procedure using carbon disulfide
9.2.5 Expression of results
57 9.3 Method B
9.3.1 Principle
9.3.2 Apparatus
9.3.3 Reagents
9.3.4 Chromatographic conditions
58 9.3.5 Preparation of calibration curve (soluble sulfur)
9.3.6 DSC programme
9.3.7 Procedure for initial soluble sulfur
59 9.3.8 Procedure for soluble sulfur after 10-min exposure time
9.3.9 Expression of results
9.4 Precision
60 10 Determination of loss in mass at 80 °C
10.1 Principle
10.2 Apparatus
10.3 Procedure
10.3.1 Method A
10.3.2 Method B
61 10.4 Expression of results
10.5 Precision
11 Determination of ash at 850 °C to 900 °C
11.1 Principle
11.2 Apparatus
11.3 Procedure
62 11.4 Expression of results
11.5 Precision
12 Determination of acidity
13 Determination of arsenic content
14 Test report
64 Annex A (informative) Typical values of the properties of sulfur used as a rubber compounding ingredient
66 Annex B (informative) Precision
69 Bibliography
BS ISO 8332:2018 - TC
$217.84