{"id":207748,"date":"2024-10-19T13:23:00","date_gmt":"2024-10-19T13:23:00","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/astm-d3559-2008-2\/"},"modified":"2024-10-25T06:04:45","modified_gmt":"2024-10-25T06:04:45","slug":"astm-d3559-2008-2","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/astm\/astm-d3559-2008-2\/","title":{"rendered":"ASTM-D3559 2008"},"content":{"rendered":"<\/p>\n
1.1 These test methods cover the determination of dissolved and total recoverable lead in water and waste water by atomic-absorption spectrophotometry and differential pulse anodic stripping voltammetry. Four test methods are included as follows:<\/p>\n
1.2 Test Method B can be used to determine lead in brines. Test Method D has been used successfully with reagent water, lake water, well water, filtered tap water, condensate from a medium Btu coal gasification process, waste treatment plant effluent, and a production plant process water.<\/p>\n
1.3 It is the user’s responsibility to ensure the validity of these test methods for waters of untested matrices.<\/p>\n
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.<\/p>\n
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazards statements, see 10.4.1, Note 2, 11.2, 11.3, 21.7, 21.8, 21.11, 23.7, 23.10, 32.2.1, and 33.1.<\/span><\/span><\/p>\n 7.1 This test method covers the determination of dissolved and total recoverable lead in most waters and wastewaters.<\/p>\n 7.2 The test method is applicable in the range from 1.0 to 10 mg\/L of lead. The upper limits of detectability can be increased to concentrations greater than 10 mg\/L by dilution of the sample.<\/p>\n 17.1 This test method covers the determination of dissolved and total recoverable lead in most waters and brines.<\/p>\n 17.2 This test method is applicable in the range from 100 to 1000 ?<\/span> g\/L of lead. The range may be extended upward by dilution of the samples.<\/p>\n 27.1 This test method describes the determination of lead in water and waste waters using differential pulse anodic stripping voltammetry.<\/p>\n 27.2 This test method is applicable up to a concentration of 100 ?<\/span> g\/L lead. Higher concentrations can be determined by dilution.<\/p>\n 27.3 The lower limit of detection for lead is 1.0 ?<\/span> g\/L.<\/p>\n Note<\/span> 13The lower limit of detection for differential pulse anodic stripping voltammetry is not absolute and can easily be lowered by changing the experimental parameters as described in Appendix X1. However, these variations have not been interlaboratory tested.<\/p>\n 39.1 This test method covers the determination of dissolved and total recoverable lead in most waters and wastewaters.<\/p>\n 39.2 The test method is applicable in the range from 5 to 100 ?<\/span> g\/L of lead using a 20- ?<\/span> L injection. The range can be increased or decreased by varying the volume of sample injected or the instrumental settings. High concentrations may be diluted but preferably should be analyzed by direct aspiration atomic absorption spectrophotometry (Test Method A).<\/p>\n 39.3 This test method has been used successfully with reagent water, lake water, river water, well water, filtered tap water, condensate from a medium Btu coal gasification process, waste treatment plant effluent, and a production plant process water. It is the user’s responsibility to assure validity of this test method for untested matrices.<\/p>\n D3559-08 Standard Test Methods for Lead in Water<\/b><\/p>\nPDF Catalog<\/h4>\n
\n
\n PDF Pages<\/th>\n PDF Title<\/th>\n<\/tr>\n \n 1<\/td>\n Scope
Referenced Documents
Terminology <\/td>\n<\/tr>\n\n 2<\/td>\n Significance and Use
Purity of Reagents
Sampling
Scope
Summary of Test Method
Interferences
Apparatus
Reagents <\/td>\n<\/tr>\n\n 3<\/td>\n Standardization
Procedure
Calculation
Precision and Bias
Quality Control
TABLE 1 <\/td>\n<\/tr>\n\n 4<\/td>\n Scope
Summary of Test Method <\/td>\n<\/tr>\n\n 5<\/td>\n Interferences
Apparatus
Reagents
Standardization
Procedure <\/td>\n<\/tr>\n\n 6<\/td>\n Calculation
Precision and Bias
Quality Control
TABLE 2 <\/td>\n<\/tr>\n\n 7<\/td>\n Scope
Terminology
Summary of Test Method
Interferences <\/td>\n<\/tr>\n\n 8<\/td>\n Apparatus
Reagents
Caution
Calibration <\/td>\n<\/tr>\n\n 9<\/td>\n Procedure
Calculation
Precision and Bias
TABLE 3 <\/td>\n<\/tr>\n\n 10<\/td>\n Quality Control <\/td>\n<\/tr>\n \n 11<\/td>\n Scope
Summary of Test Method
Interferences
Apparatus
Reagents
TABLE 4
TABLE 5 <\/td>\n<\/tr>\n\n 12<\/td>\n Standardization
Procedure
Calculation
Precision and Bias
Quality Control <\/td>\n<\/tr>\n\n 13<\/td>\n Keywords <\/td>\n<\/tr>\n \n 14<\/td>\n A1. PROCEDURE TO CLEAN GLASSWARE
A1.1
A1.2
A1.3
A2. DETERMINATION OF HANGING MERCURY DROP AREA
A2.1
A2.2
A2.3
A2.4
A2.5
A2.6
A2.7
A2.8 <\/td>\n<\/tr>\n\n 15<\/td>\n X1. THE SENSITIVITY OF DIFFERENTIAL PULSE ANODIC STRIPPING VOLTAMMETRY
X1.1
X1.2
X1.3
X1.4
X1.5
X1.6
X1.7
X2. METHODS FOR REMOVING OXYGEN FROM NITROGEN GAS
X2.1 <\/td>\n<\/tr>\n\n 16<\/td>\n X3. CHEMICAL MATRIX MODIFIERS FOR LEAD DETERMINATIONS USING GRAPHITE FURNACE SPECTROPHOTOMETRY
X3.1
TABLE X3.1 <\/td>\n<\/tr>\n\n 17<\/td>\n X4. VOLTAMMOGRAM
X4.1
FIG. X4.1 <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"\n\n
\n Published By<\/td>\n Publication Date<\/td>\n Number of Pages<\/td>\n<\/tr>\n \n ASTM<\/b><\/a><\/td>\n 2008<\/td>\n 17<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":207751,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[216,2637],"product_tag":[],"class_list":{"0":"post-207748","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-13-060-50","7":"product_cat-astm","9":"first","10":"instock","11":"sold-individually","12":"shipping-taxable","13":"purchasable","14":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/207748","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/207751"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=207748"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=207748"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=207748"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}