{"id":303106,"date":"2024-10-19T20:42:58","date_gmt":"2024-10-19T20:42:58","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bsi-pd-iec-ts-62607-6-132020\/"},"modified":"2024-10-25T18:15:04","modified_gmt":"2024-10-25T18:15:04","slug":"bsi-pd-iec-ts-62607-6-132020","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bsi-pd-iec-ts-62607-6-132020\/","title":{"rendered":"BSI PD IEC TS 62607-6-13:2020"},"content":{"rendered":"

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
2<\/td>\nundefined <\/td>\n<\/tr>\n
4<\/td>\nCONTENTS <\/td>\n<\/tr>\n
6<\/td>\nFOREWORD <\/td>\n<\/tr>\n
8<\/td>\nINTRODUCTION <\/td>\n<\/tr>\n
9<\/td>\n1 Scope
2 Normative references
3 Terms, definitions, symbols and abbreviated terms <\/td>\n<\/tr>\n
10<\/td>\n3.1 Terms and definitions
3.1.1 General terms <\/td>\n<\/tr>\n
11<\/td>\n3.1.2 Key control characteristics measured according to this document
oxygen functional group
3.1.3 Terms related to the measurement method
3.2 Symbols and abbreviated terms
4 General
4.1 Measurement principle <\/td>\n<\/tr>\n
12<\/td>\n4.2 Sample preparation method
Figures
Figure 1 \u2013 Test principle of Boehm titration
Tables
Table 1 \u2013 Four types of oxygen functional group and their structures <\/td>\n<\/tr>\n
13<\/td>\n4.3 Description of measurement equipment \/ apparatus
4.3.1 Analytical balance, readability is 0,1 mg.
4.3.2 Electric thermostatic drying oven
4.3.3 Numerical control magnetic agitator\/oscillator
4.3.4 Automatic potentiometer, with pH electrode and accurate to 0,1 mV.
4.3.5 HDPE bottles, the volume are 1 000 mL and 100 mL, with stopper.
4.4 Supporting materials
4.5 Ambient conditions during measurement
5 Measurement procedure
5.1 Detailed protocol of the measurement procedure
5.1.1 Preparation of solutions
Table 2 \u2013 Reagents used in this document <\/td>\n<\/tr>\n
15<\/td>\n5.1.2 Reactions between graphene and bases
5.1.3 Instrument preparation
5.1.4 Titration of the filtrate <\/td>\n<\/tr>\n
16<\/td>\n5.2 Measurement uncertainty
5.3 Operation procedure, key control steps and case study
6 Data analysis \/ interpretation of results
6.1 Normalized base consumption <\/td>\n<\/tr>\n
17<\/td>\n6.2 Oxygen functional group content
7 Results to be reported
7.1 General
7.2 Product\/sample identification
7.3 Test results <\/td>\n<\/tr>\n
18<\/td>\nAnnex A (informative)Operation procedure and key control steps
A.1 Operation procedure
Figure A.1 \u2013 Operation procedure <\/td>\n<\/tr>\n
19<\/td>\nA.2 Key control steps
Figure A.2 \u2013 Key control steps <\/td>\n<\/tr>\n
20<\/td>\nAnnex B (informative)Influence of CO2
B.1 Effect of CO2 on titration of base concentration
Figure B.1 \u2013 Titration curves of NaOH solution <\/td>\n<\/tr>\n
21<\/td>\nB.2 Effect of CO2 on base consumption
Table B.1 \u2013 Titration results of back titration and direct titration of NaOH solution
Table B.2 \u2013 Results of base consumption of NaOH with and without bubbling N2 <\/td>\n<\/tr>\n
22<\/td>\nAnnex C (informative)Lower limit of determination
C.1 Experiment of lower mass of reacted sample A
C.2 Determination of detection limits
Figure C.1 \u2013 The normalized base consumption of different amounts of sample A <\/td>\n<\/tr>\n
23<\/td>\nTable C.1 \u2013 Base consumption result of sample A <\/td>\n<\/tr>\n
24<\/td>\nTable C.2 \u2013 Oxygen functional group content result
Table C.3 \u2013 Detection limits for different sample amounts <\/td>\n<\/tr>\n
25<\/td>\nAnnex D (informative)Test report
D.1 Example of a test record
D.2 Format of the test report
Table D.1 \u2013 Data for calibration of titrant acid
Table D.2 \u2013 Data for Boehm titration <\/td>\n<\/tr>\n
26<\/td>\nTable D.3 \u2013 Product identification (according to IEC 62565-3-1)
Table D.4 \u2013 General material description (according to IEC 62565-3-1)
Table D.5 \u2013 Measurement results <\/td>\n<\/tr>\n
27<\/td>\nAnnex E (informative)Case study
E.1 Preparation of solution
E.2 Sample preparation
E.3 Reactions between graphene and bases <\/td>\n<\/tr>\n
28<\/td>\nE.4 Titration of the filtrate <\/td>\n<\/tr>\n
29<\/td>\nFigure E 1 \u2013 Titration curves of A0 filtrate (upper left), B0 filtrate (upper right), C0 filtrate (lower left), and D0 filtrate (lower right)
Table E.1 \u2013 Measurement data <\/td>\n<\/tr>\n
30<\/td>\nE.5 Calculation <\/td>\n<\/tr>\n
31<\/td>\nTable E.2 \u2013 Normalized base consumption of sample 1 <\/td>\n<\/tr>\n
32<\/td>\nE.6 Test report
Table E.3 \u2013 Product identification of sample 1
Table E.4 \u2013 General material description of sample 1
Table E.5 \u2013 Measurement results of sample 1 <\/td>\n<\/tr>\n
33<\/td>\nBibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

Nanomanufacturing. Key control characteristic – Graphene powder. Oxygen functional group content: Boehm titration method<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
BSI<\/b><\/a><\/td>\n2020<\/td>\n36<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":303115,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[2641],"product_tag":[],"class_list":{"0":"post-303106","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-bsi","8":"first","9":"instock","10":"sold-individually","11":"shipping-taxable","12":"purchasable","13":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/303106","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/303115"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=303106"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=303106"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=303106"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}