{"id":402709,"date":"2024-10-20T05:02:32","date_gmt":"2024-10-20T05:02:32","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bsi-pd-cen-ts-17784-12022\/"},"modified":"2024-10-26T08:58:39","modified_gmt":"2024-10-26T08:58:39","slug":"bsi-pd-cen-ts-17784-12022","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bsi-pd-cen-ts-17784-12022\/","title":{"rendered":"BSI PD CEN\/TS 17784-1:2022"},"content":{"rendered":"
This document specifies two methods required for the identification of lignosulfonate by UV-Vis spectrophotometry (method A) and gravimetry (method B) in organo-mineral fertilizers. NOTE Lignosulfonate, as a complexing agent, is a natural polymer produced as a by-product of the sulfite method for manufacturing paper from wood pulp in the paper industry. As a natural polymer, it presents a poorly defined and variable chemical structure. It is an intricate mixture of small- to moderate-sized polymeric compounds with sulfonate groups attached to the molecule, and diverse complexing capacity.<\/p>\n
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7<\/td>\n | 1 Scope 2 Normative references 3 Terms and definitions 4 Sampling and sample preparation 5 Method A: Determination of phenolic hydroxyl content and 232,5 nm absorbance for the identification of lignosulfonates 5.1 Principle <\/td>\n<\/tr>\n | ||||||
8<\/td>\n | 5.2 Reagents 5.3 Apparatus <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 5.4 Procedure 5.4.1 Preparation of stock solution 5.4.2 Solution A (acid) 5.4.3 Solution B (basic) 5.4.4 Solution C 5.4.5 Measurement of phenolic hydroxyl content 5.4.6 Measurement of 232,5 nm absorbance 5.5 Calculation 5.5.1 Phenolic hydroxyl content <\/td>\n<\/tr>\n | ||||||
11<\/td>\n | 5.5.2 Lignosulfonic acid content calculated from 232,5 nm absorbance 6 Method B: Determination of organic sulfur content for the identification of lignosulfonates 6.1 Principle 6.2 Reagents <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | 6.3 Apparatus <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | 6.4 Procedure 6.4.1 Preparation of 0,5 mol\/l Iodine I2 solution 6.4.2 Separation of inorganic sulfur 6.4.3 Determination of organic sulfur <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | 6.5 Calculation 7 Expression of the results 7.1 Relative phenolic hydroxyl content <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | 7.2 Relative organic sulfur content 8 Test report <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Organo-mineral fertilizers. Identification of complexing agents. – Method using UV-Vis spectrophotometry and gravimetry<\/b><\/p>\n |