BSI PD CEN/TS 17197:2018:2019 Edition

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Construction products: Assessment of release of dangerous substances. Analysis of inorganic substances in digests and eluates. Analysis by Inductively Coupled Plasma. Optical Emission Spectrometry (ICP-OES)

Published By	Publication Date	Number of Pages
BSI	2019	36

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Categories: 91.100.01 - Construction materials in general, BSI

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This Technical Specification specifies the method for the determination of major, minor and trace elements in aqua regia and nitric acid digests and in eluates of construction products by Inductively Coupled Plasma – Optical Emission Spectrometry (ICP-OES). It refers to the following 44 elements: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), phosphorus (P), potassium (K), praseodymium (Pr), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulphur (S), tellurium (Te), thallium (Tl), thorium (Th), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), zinc (Zn), and zirconium (Zr). For the determination of low levels of As, Se and Sb, hydride generation may be applied. This method is described in Annex D. NOTE Construction products include e.g. mineral-based products (S); bituminous products (B); metals (M); wood-based products (W); plastics and rubbers (P); sealants and adhesives (A); paints and coatings (C), see also CEN/TR 16045 [1]. The method in this Technical Specification is applicable to construction products and validated for the product types listed in Annex D.

PDF Catalog

PDF Pages	PDF Title
2	National foreword
6	European foreword
7	Introduction
8	1 Scope 2 Normative references 3 Terms and definitions
10	4 Symbols and abbreviations 5 Principle 6 Interferences
11	7 Reagents 7.1 General
12	7.5 Single-element standard stock solutions 7.6 Multi-element standard stock solutions 7.6.1 General 7.7 Multi-element calibration solutions
13	7.8 Internal standard solution 7.9 Calibration blank 7.10 Method blank 7.11 Calibration check solution 7.12 Interference check solution (ICS) 8 Apparatus 8.1 Inductively coupled argon plasma emission spectrometer
14	8.2 Volumetric flasks 8.3 Volumetric pipets 9 Procedure 9.1 Test sample 9.2 Test portion 9.3 Instrument set up 9.3.1 General requirements
15	9.3.2 Inter-element correction 9.3.3 Internal standard 9.3.4 Instrument performance check 9.4 Calibration 9.4.1 Linear calibration function
16	9.4.2 Non-linear calibration function 9.4.3 Standard addition calibration 9.5 Sample measurement
17	10 Calculation 10.1 Calculation for digests of construction products 10.2 Calculation for eluates of construction products 11 Expression of results 12 Performers characteristics 12.1 General 12.2 Blank 12.3 Calibration check 12.4 Interference
18	12.5 Recovery 12.6 Precision
19	13 Test report
21	Annex A (informative) Wavelengths, spectral interferences and estimated method detection limits
24	Annex B (informative) Method detection limit (MDL) and precision data for soil, sludge and biowaste
27	Annex C (informative) Inter element correction (IEC)
29	Annex D (normative) Determination of arsenic, antimony and selenium using hydride-generation ICP-OES
33	Bibliography