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ASTM-D1552:2008 Edition

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D1552-08 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)

Published By Publication Date Number of Pages
ASTM 2008 7
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ASTM D1552-08

Historical Standard: Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)

ASTM D1552

Scope

1.1 This test method covers three procedures for the determination of total sulfur in petroleum products including lubricating oils containing additives, and in additive concentrates. This test method is applicable to samples boiling above 177Ā°C (350Ā°F) and containing not less than 0.06 mass % sulfur. Two of the three procedures use iodate detection; one employing an induction furnace for pyrolysis, the other a resistance furnace. The third procedure uses IR detection following pyrolysis in a resistance furnace.

1.2 Petroleum coke containing up to 8 mass % sulfur can be analyzed.

1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Keywords

furnace; high temperature; induction furnace; iodate titration; IR detection; petroleum; resistance; sulfur; titration; Fuel sulfur; High-temperature processing/testing; Petroleum products

ICS Code

ICS Number Code 75.080 (Petroleum products in general)

DOI: 10.1520/D1552-08

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Summary of Test Method
Significance and Use
Interferences
2 Apparatus
Reagents and Materials
FIG. 1
3 Sampling
Preparation of Apparatus
Standardization
FIG. 2
TABLE 1
4 Preparation of Coke
Analysis of Quality Control Samples
Procedure with Induction-Type Furnace
FIG. 3
TABLE 2
5 Procedure with Resistance-Type Furnace
Procedure with Resistance Furnaceā€“IR Detection
Calculation
Report
Quality Control
Precision and Bias
6 Keywords
X1. QUALITY CONTROL
X1.1
X1.2
X1.3
X1.4
X1.5
7 X1.6
ASTM-D1552
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