ASTM-D6228 2003

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D6228-98(2003) Standard Test Method for Determination of Sulfur Compounds in Natural Gas and Gaseous Fuels by Gas Chromatography and Flame Photometric Detection

Published By	Publication Date	Number of Pages
ASTM	2003	6

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Categories: 71.040.50 - Physicochemical methods of analysis, ASTM

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Description

ASTM D6228-98-Reapproved2003

Historical Standard: Standard Test Method for Determination of Sulfur Compounds in Natural Gas and Gaseous Fuels by Gas Chromatography and Flame Photometric Detection

ASTM D6228

Scope

1.1 This test method covers the determination of individual volatile sulfur-containing compounds in gaseous fuels by gas chromatography (GC) with flame photometric detection (FPD). The detection range for sulfur compounds is from 20 to 20 000 picograms (pg) of sulfur. This is equivalent to 0.02 to 20 mg/m³ or 0.014 to 14 ppmv of sulfur based upon the analysis of a 1-mL sample.

1.2 This test method describes a GC-FPD method using a specific capillary GC column. Other GC-FPD methods, with differences in GC column and equipment setup and operation, may be used as alternative methods for sulfur compound analysis with different range and precision, provided that appropriate separation of the sulfur compounds of interest can be achieved.

1.3 This test method does not intend to identify all individual sulfur species. Total sulfur content of samples can be estimated from the total of the individual compounds determined. Unknown compounds are calculated as monosulfur-containing compounds.

1.4 The values stated in SI units are to be regarded as standard. The values stated in inch-pound units are for information only.

1.5 This standard does not purport to address all the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Keywords

flame photometric detection; gas chromatography; sulfur compounds, odorants

ICS Code

ICS Number Code 71.040.50 (Physicochemical methods of analysis)

DOI: 10.1520/D6228-98R03

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents Terminology
2	Summary of Test Method Significance and Use Apparatus
3	Reagents and Materials Preparation of Apparatus and Calibration TABLE 1
4	Procedure TABLE 2
5	Calculation Report Precision and Bias FIG. 1 TABLE 3
6	Keywords

Additional information

Standard Title	D6228-98(2003) Standard Test Method for Determination of Sulfur Compounds in Natural Gas and Gaseous Fuels by Gas Chromatography and Flame Photometric Detection
Published Code	ASTM
Publication Date	2003
Pages Count	6
ICS Codes	71.040.50 - Physicochemical methods of analysis