{"id":205484,"date":"2024-10-19T13:11:43","date_gmt":"2024-10-19T13:11:43","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/astm-c997-1993\/"},"modified":"2024-10-25T05:51:50","modified_gmt":"2024-10-25T05:51:50","slug":"astm-c997-1993","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/astm\/astm-c997-1993\/","title":{"rendered":"ASTM-C997 1993"},"content":{"rendered":"

ASTM C997-83-e1-Reapproved1993<\/h3>\n

Withdrawn Standard: Test Methods for Chemical and Instrumental Analysis of Nuclear-Grade Sodium and Cover Gas (Withdrawn 1999)<\/h4>\n
\n

ASTM C997<\/h4>\n

Scope<\/strong><\/p>\n

1.1 These test methods provide instructions for performing chemical, radiochemical, and instrumental analyses of sodium metal and for determining impurities in cover gas.<\/p>\n

1.2 The analytical procedures appear in the following order:<\/p>\n

Sections Bypass Sampling 6 to 12 Overflow Sampling 13 to 18 Wire and Foil Equilibration Sampling 19 to 24 Laboratory Distillation of Sodium 25 to 31 Hydrogen by Hydrogen-Diffusion Meter 32 to 37 Carbon by Oxyacidic-Flux Method 38 to 46 Carbonaceous Gases Released by Acid 47 to 54 Cyanide by Spectrophotometry 55 to 64 Oxygen by the Equilibration Method Using Vanadium Wires 65 to 74 Fluoride by Selective Ion Electrode 75 to 83 Chloride by Selective Ion Electrode 84 to 92 Trace Metals by Atomic Absorption or Flame Emission 93 to 101 Spectrophotometry Cadmium and Zinc by Atomic Absorption Spectrophotometry 102 to 111 Potassium by Atomic Absorption Spectrophotometry 112 to 121 Rubidium and Cesium by Flame Spectrometry 122 to 131 Silicon by Spectrophotometry 132 to 140 Boron by Spectrophotometry 141 to 149 Uranium by Fluorimetry 150 to 157 Oxygen by Oxygen Meter 158 to 164 Carbon by Equilibration Method 165 to 172 Hydrogen by Equilibration Method 173 to 180 Sulfur by Spectrophotometry 181 to 189 Sodium Purity By Titration 190 to 199 Plutonium by Alpha Assay 200 to 209 Gamma Assay of Distillation Residue 210 to 217 Gamma Assay of Sodium Solution 218 to 226 Radioactive Iodine by Gamma Counting 227 to 235 Tritium by Liquid Scintillation Counting 236 to 245 Particles by Filtration 246 to 254 Gaseous Impurities in Cover Gas by Gas Chromatography 255 to 263<\/p>\n

Keywords<\/strong><\/p>\n

Boron content-nuclear-grade materials; Cadmium content; Carbon content-nuclear materials; Cesium content; Chloride content-nuclear applications; Cyanides content; Distillation; Fluoride content; Gamma radiation; Gas chromatography-nuclear; Gases-radioactive; Hydrogen content-nuclear materials; Impurities-nuclear materials; Iodine-radioactive; Nuclear fuels (reactor); Oxygen content; Plutonium-isotopic analysis; Potassium content; Rubidium content; Sampling-nuclear\/related energy sources; Silicon content; Sodium-nuclear applications; Solids content; Sulfur content-nuclear materials; Trace elements content-nuclear materials; Tritium content; Uranium content; Zinc content; sodium\/cover gas (nuclear-grade)- chemical\/instrumental analysis,; methods<\/p>\n

ICS Code<\/strong><\/p>\n

ICS Number Code 27.120.30 (Fissile materials and nuclear fuel technology)<\/p>\n

DOI:<\/strong><\/p>\n<\/div>\n

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
1<\/td>\nScope
Referenced Documents
Significance and Use
Reagents
Safety Precautions <\/td>\n<\/tr>\n
2<\/td>\nScope
Summary of Method
Apparatus
Reagents and Materials
Precautions
Procedure
FIG. 1 <\/td>\n<\/tr>\n
3<\/td>\nDiscussion
Scope
Summary of Method
Apparatus
TABLE 1
FIG. 2 <\/td>\n<\/tr>\n
4<\/td>\nPrecautions
Procedure
FIG. 3
FIG. 4 <\/td>\n<\/tr>\n
5<\/td>\nFIG. 5 <\/td>\n<\/tr>\n
6<\/td>\nDiscussion
Scope
Summary of Method
Apparatus <\/td>\n<\/tr>\n
7<\/td>\nPrecautions
Procedure
Discussion
Scope
Summary of Method
Apparatus
Reagents and Materials
FIG. 6 <\/td>\n<\/tr>\n
8<\/td>\nPrecautions
Procedure
FIG. 7 <\/td>\n<\/tr>\n
9<\/td>\nDiscussion
FIG. 8
FIG. 9 <\/td>\n<\/tr>\n
10<\/td>\nScope
Summary of Method
Apparatus
Procedure
FIG. 10
FIG. 11 <\/td>\n<\/tr>\n
11<\/td>\nCalculation
Precision and Accuracy
Scope
Summary of Method
Apparatus
FIG. 12 <\/td>\n<\/tr>\n
12<\/td>\nFIG. 13
FIG. 14
FIG. 15 <\/td>\n<\/tr>\n
13<\/td>\nReagents and Materials
Preparation of Apparatus
Calibration of Chromatograph
FIG. 16
FIG. 17 <\/td>\n<\/tr>\n
14<\/td>\nProcedure
FIG. 18 <\/td>\n<\/tr>\n
15<\/td>\nCalculation
Precision and Accuracy
Scope
Summary of Method
Apparatus <\/td>\n<\/tr>\n
16<\/td>\nReagents and Materials
Calibration of Chromatograph
Procedure
FIG. 19
FIG. 20 <\/td>\n<\/tr>\n
17<\/td>\nFIG. 21
FIG. 22 <\/td>\n<\/tr>\n
18<\/td>\nCalculation
Precision and Accuracy
Scope
Summary of Method
Interferences
Apparatus
FIG. 23 <\/td>\n<\/tr>\n
19<\/td>\nReagents and Materials
Precautions
Calibration
Procedure <\/td>\n<\/tr>\n
20<\/td>\nCalculation
Precision and Accuracy
Scope
Summary of Method
Interferences
Apparatus
FIG. 24 <\/td>\n<\/tr>\n
21<\/td>\nReagents and Materials
Precautions
Calibration of Vacuum-Fusion Analyzer
Procedure
FIG. 25
FIG. 26 <\/td>\n<\/tr>\n
22<\/td>\nTABLE 2 <\/td>\n<\/tr>\n
23<\/td>\nCalculation
Precision and Accuracy <\/td>\n<\/tr>\n
24<\/td>\nScope
Summary of Method
Interferences
Apparatus
Reagents and Materials
Calibration
Procedure
TABLE 3 <\/td>\n<\/tr>\n
25<\/td>\nCalculation
Precision and Accuracy
Scope
Summary of Method
Interferences
Apparatus
Reagents and Materials
Calibration
Procedure
Calculation <\/td>\n<\/tr>\n
26<\/td>\nPrecision and Accuracy
Scope
Summary of Method
Apparatus
Reagents and Materials
TABLE 4 <\/td>\n<\/tr>\n
27<\/td>\nPrecautions
Calibration
Procedure
TABLE 5 <\/td>\n<\/tr>\n
28<\/td>\nCalculation
Precision and Accuracy
Scope
Summary of Method
Interferences
Apparatus
Reagents and Materials
Precautions
TABLE 6 <\/td>\n<\/tr>\n
29<\/td>\nCalibration
Procedure
Calculation
Precision and Accuracy
Scope
Summary of Method
Interferences
Apparatus
Reagents and Materials <\/td>\n<\/tr>\n
30<\/td>\nPrecautions
Calibration
Procedure
Calculation
Precision and Accuracy
Scope <\/td>\n<\/tr>\n
31<\/td>\nSummary of Method
Interferences
Apparatus
Reagents and Materials
Precautions
Calibration
Procedure <\/td>\n<\/tr>\n
32<\/td>\nCalculation
Precision and Accuracy
Scope
Summary of Method
Interferences
Apparatus
Reagents and Materials
Calibration <\/td>\n<\/tr>\n
33<\/td>\nProcedure
Calculation
Precision and Accuracy
Scope
Summary of Method
Interferences
Apparatus
Reagents and Materials <\/td>\n<\/tr>\n
34<\/td>\nCalibration
Procedure
Calculation
Precision and Accuracy
Scope
Summary of Method
Apparatus
Reagents and Materials <\/td>\n<\/tr>\n
35<\/td>\nCalibration
Procedure
Calculation
Precision and Accuracy
Scope
Summary of Method
Apparatus
Precautions <\/td>\n<\/tr>\n
36<\/td>\nCalibration
Procedure
Precision and Accuracy
Scope
Summary of Method
Apparatus
Reagents and Materials
FIG. 27 <\/td>\n<\/tr>\n
37<\/td>\nCalibration
Procedure
Calculation
Precision and Accuracy
Scope
Summary of Method
Apparatus <\/td>\n<\/tr>\n
38<\/td>\nReagents and Materials
Calibration
Procedure
Calculation
Precision and Accuracy
Scope
Summary of Method
Apparatus <\/td>\n<\/tr>\n
39<\/td>\nReagents and Materials
Precautions
Calibration
Procedure
Calculation
FIG. 28 <\/td>\n<\/tr>\n
40<\/td>\nPrecision and Accuracy
Scope
Summary of Method
Interferences
Apparatus
Reagents and Materials
Precautions
Calibration
Procedure <\/td>\n<\/tr>\n
41<\/td>\nCalculation <\/td>\n<\/tr>\n
42<\/td>\nPrecision and Accuracy
Scope
Summary of Method
Interferences
Apparatus
Reagents and Materials <\/td>\n<\/tr>\n
43<\/td>\nPrecautions
FIG. 29
FIG. 30 <\/td>\n<\/tr>\n
44<\/td>\nCalibration
Procedure
FIG. 31 <\/td>\n<\/tr>\n
45<\/td>\nCalculation
Precision and Accuracy
Scope
Summary of Method
Apparatus
Reagents and Materials
Calibration
Procedure
Calculation
Precision and Accuracy
Scope <\/td>\n<\/tr>\n
46<\/td>\nSummary of Method
Apparatus
Reagents and Materials
Precautions
Calibration
Procedure
Calculation
Precision and Accuracy
Scope
Summary of Method <\/td>\n<\/tr>\n
47<\/td>\nApparatus
Reagents and Materials
Precautions
Calibration
Procedure
Calculation <\/td>\n<\/tr>\n
48<\/td>\nPrecision and Accuracy
Scope
Summary of Method
Interferences
Apparatus
Reagents and Materials
Precautions
Calibration
Procedure <\/td>\n<\/tr>\n
49<\/td>\nCalculation
Precision and Accuracy
Scope
Summary of Method
Apparatus
FIG. 32 <\/td>\n<\/tr>\n
50<\/td>\nReagents and Materials
Precleaning and Testing
Sampling
Procedure
Calculation
Precision and Accuracy
Scope <\/td>\n<\/tr>\n
51<\/td>\nSummary of Method
Apparatus
TABLE 7 <\/td>\n<\/tr>\n
52<\/td>\nReagents and Materials
Precautions
Calibration
Procedure
FIG. 33 <\/td>\n<\/tr>\n
53<\/td>\nCalculation
Precision and Accuracy
Keywords
REFERENCES <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

C997-83(1993)e1 Test Methods for Chemical and Instrumental Analysis of Nuclear-Grade Sodium and Cover Gas (Withdrawn 1999)<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
ASTM<\/b><\/a><\/td>\n1993<\/td>\n53<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":205492,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[464,2637],"product_tag":[],"class_list":{"0":"post-205484","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-27-120-30","7":"product_cat-astm","9":"first","10":"instock","11":"sold-individually","12":"shipping-taxable","13":"purchasable","14":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/205484","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/205492"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=205484"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=205484"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=205484"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}